ChansonRolandV6, Main, Exploration, bibRecord, 000653

Application of the heck reaction for the synthesis of 1-alkoxyisoquinoline- 3-carboxylic acids esters

Identifieur interne : 000653 ( Main/Exploration ); précédent : 000652; suivant : 000654

Application of the heck reaction for the synthesis of 1-alkoxyisoquinoline- 3-carboxylic acids esters

Auteurs : A. Ture [Lettonie] ; K. Rubina [Lettonie] ; E. Rozhkov [Lettonie] ; V. Kauss [Lettonie]

Source :

Chemistry of Heterocyclic Compounds [ 0009-3122 ] ; 2011.

RBID : ISTEX:BCC26459804A6A191B94FD0BCF1BF37473ECF675

English descriptors

Teeft :
- Acid ester, Acrylate, Argon atmosphere, Cdcl3, Chem, Co2me, Column chromatography, Corresponding acid ester, Doctoral study, Ester, Ethyl acetate, Heck, Heck reaction, Heterogeneous mixture, Irel, Mass spectrum, Methyl, Mmol, Och3, Organic phase, Palladium diacetate, Reaction mixture, Reaction product, Room temperature, Sodium bicarbonate, Sodium chloride solution, Sodium sulfate, Suzuki reaction, Tetrabutylammonium bromide, Tetrahedron lett, Varian instrument, White powder.

Abstract

It has been shown that the cyclization of the methyl 2-(2,2,2-trifluoroacetylamino)acrylate arylation product using methyl 4,6-dichloro-2-iodobenzoate gives the corresponding 1-methoxyisoquinoline-3-carboxylic acid ester through loss of water rather than methanol. This feature of the condensation has been used for the synthesis of methyl 1-(tert-butoxycarbonylmethoxy)isoquinoline-3-carboxylate.

Url:

https://api.istex.fr/ark:/67375/VQC-2GJ3LT8L-D/fulltext.pdf

DOI: 10.1007/s10593-011-0844-7

Affiliations:

Lettonie

Links toward previous steps (curation, corpus...)

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to stream Istex, to step Curation: 001712
to stream Istex, to step Checkpoint: 000614
to stream Main, to step Merge: 000655
to stream Main, to step Curation: 000653

Le document en format XML

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<front><div type="abstract" xml:lang="en">It has been shown that the cyclization of the methyl 2-(2,2,2-trifluoroacetylamino)acrylate arylation product using methyl 4,6-dichloro-2-iodobenzoate gives the corresponding 1-methoxyisoquinoline-3-carboxylic acid ester through loss of water rather than methanol. This feature of the condensation has been used for the synthesis of methyl 1-(tert-butoxycarbonylmethoxy)isoquinoline-3-carboxylate.</div>
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Application of the heck reaction for the synthesis of 1-alkoxyisoquinoline- 3-carboxylic acids esters

Application of the heck reaction for the synthesis of 1-alkoxyisoquinoline- 3-carboxylic acids esters

Source :

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

Pour mettre un lien sur cette page dans le réseau Wicri